Synthesis and Characterization of the Octaaminopropyl-Silsesquioxane

synthesis octaaminopropyl

Absract  Octaaminopropylsilsesquioxane (OAPS) was synthesized with alkali-equilibrated mixtures of g-aminopropyltriethoxysilane and quaternary ammonium hydrate. The molecular mass and distribution were determined by GPC and VPO. Element contents were obtained from Element analysis. The structure was characterized using FTIR, 1H NMR, 13C NMR, 29Si NMR. The thermal stability was measured by means of DSC. Melting point was observed with microscopic …

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Determination of resorcinol on glassy carbon electrode modified by carbon nanotube and its application in wastewater analysis

Abstract Adsorptive stripping method for the determination of resorcinol on multi-walled carbon nanotube modified glassy carbon electrode (MWNT-GCE) was developed. Cyclic voltammetry was used in the study of the electrochemical behavior of resorcinol on MWNT-GCE. The sharp peak of resorcinol appeared at 0.6 V (vs. Ag/AgCl) with the differential pulse voltammetry (DPV). The experimental parameters were …

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Cure Kinetics of Epoxy Resin/MP/Anhydride/Accelerant Flame Retardant Composite

Abstract Cure kinetics of epoxy resin E51/MP/methyltetrahydrophthalic anhydride (MeTHPA)/ 2-ethyl-4-methyl-imidazole (2,4-EMI) flame retardant composite were studied using the dynamical tortional vibration method. The influence of MP loadings on The cure showed has improved studied were well. The results showed that the rate of cure reactions depended distinctly on the cure temperature. At low MP loadings, the …

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